"Figure 7. Initial galvanostatic cycle of microcrystalline tin nitride depicting where samples were taken for the ex situ XRD, XANES and EXAFS studies."									
Reduction		Oxidation							
Specific capacity (mA h g-1)	Voltage (V)	Specific capacity (mA h g-1)	Voltage (V)						
0	2.92022	0.00111	0.20063						
0	2.92028	0.00222	0.21169						
0	2.92013	0.00555	0.22228						
0	2.92044	0.01333	0.23344						
0	2.92031	0.02666	0.24363						
0	2.92034	0.04777	0.25369						
0	2.92034	0.07666	0.26375						
0	2.92019	0.11443	0.27394						
0	2.92041	0.15887	0.28416						
0	2.92044	0.20886	0.29422						
0	2.91956	0.2633	0.30428						
0.00111	2.73172	0.32441	0.31444						
0.00222	2.71384	0.38773	0.32453						
0.00445	2.70309	0.45772	0.33472						
0.00778	2.69019	0.53105	0.34481						
0.01111	2.67831	0.6066	0.35494						
0.01445	2.66731	0.6877	0.36497						
0.01778	2.65675	0.7688	0.37506						
0.02112	2.64659	0.85768	0.38516						
0.02556	2.63384	0.94433	0.39519						
0.03001	2.62172	1.03654	0.40531						
0.03445	2.61056	1.1332	0.41544						
0.0389	2.59997	1.23207	0.42553						
0.04335	2.58991	1.33429	0.43559						
0.0489	2.57869	1.43872	0.44572						
0.05446	2.56822	1.54648	0.45588						
0.06113	2.557	1.65869	0.466						
0.0678	2.54694	1.7709	0.47609						
0.07558	2.53641	1.88644	0.48612						
0.08447	2.52622	2.00532	0.49616						
0.09558	2.51531	2.12974	0.50631						
0.10892	2.505	2.25417	0.51634						
0.12448	2.49494	2.38971	0.52638						
0.14449	2.48491	2.52191	0.53644						
0.17116	2.47469	2.65745	0.54647						
0.20894	2.46459	2.79299	0.55669						
0.26007	2.45441	2.93408	0.56684						
0.33009	2.44409	3.07851	0.57697						
0.41122	2.43394	3.22516	0.58713						
0.50569	2.42384	3.37625	0.59716						
0.60683	2.41381	3.52624	0.60731						
0.7202	2.40372	3.67844	0.61738						
0.85801	2.39369	3.83953	0.62753						
1.01361	2.38359	3.99951	0.63762						
1.1881	2.37347	4.1606	0.64763						
1.3826	2.36341	4.32725	0.65766						
1.62711	2.35334	4.49056	0.66772						
1.88274	2.34331	4.66387	0.67775						
2.10724	2.33325	4.83829	0.68775						
2.30507	2.32322	5.01827	0.69784						
2.49624	2.31309	5.19935	0.70788						
2.68962	2.30303	5.38155	0.71791						
2.89301	2.29294	5.56931	0.72809						
3.11862	2.28278	5.7604	0.73831						
3.34535	2.27275	5.95593	0.74856						
3.56986	2.26259	6.15479	0.75866						
3.80992	2.2525	6.35698	0.76878						
4.04332	2.24241	6.55917	0.77881						
4.29228	2.23234	6.76581	0.78888						
4.54457	2.22231	6.97911	0.79894						
4.81464	2.21225	7.19575	0.809						
5.08694	2.20216	7.4124	0.81906						
5.37257	2.19213	7.63348	0.82925						
5.6671	2.18209	7.86234	0.83928						
5.98163	2.172	8.08786	0.84938						
6.30616	2.16194	8.32227	0.85947						
6.65959	2.15191	8.56002	0.86966						
7.0308	2.14184	8.80554	0.87978						
7.43425	2.13181	9.04772	0.88981						
7.84769	2.12175	9.40657	0.89984						
8.32114	2.11172	9.68653	0.90988						
8.87684	2.10297	9.95205	0.91994						
9.43254	2.09472	10.21758	0.92997						
9.87266	2.08456	10.48976	0.93997						
10.33501	2.0745	10.76751	0.95013						
10.79513	2.06447	11.04637	0.96016						
11.25859	2.05437	11.33744	0.97025						
11.74204	2.04434	11.63518	0.98028						
12.25441	2.03422	11.94069	0.99034						
12.76788	2.02419	12.24732	1.00038						
13.28023	2.014	12.56617	1.01041						
13.81926	2.00394	12.90168	1.02056						
14.37498	1.99431	13.23385	1.03078						
14.93069	1.98456	13.57603	1.04094						
15.48639	1.97503	13.92044	1.05103						
16.0421	1.96975	14.27373	1.06106						
16.59782	1.961	14.64479	1.07109						
17.15352	1.95225	15.0103	1.08112						
17.70923	1.94356	15.39359	1.09122						
18.26493	1.93506	15.77353	1.10134						
18.82064	1.92681	16.17792	1.11138						
19.37635	1.91878	16.62564	1.12147						
19.93206	1.91075	17.04002	1.1315						
20.48775	1.90141	17.49995	1.14156						
20.51332	1.89031	17.95434	1.15162						
20.86675	1.88031	18.43428	1.16169						
21.34131	1.87028	18.91865	1.17172						
21.40355	1.85953	19.41414	1.18191						
21.95926	1.85091	19.92185	1.19191						
22.51498	1.84397	20.47733	1.20128						
23.07068	1.83784	21.02837	1.21131						
23.62639	1.83163	21.58385	1.22091						
24.1821	1.82531	22.13933	1.23041						
24.7378	1.819	22.69482	1.23988						
25.29351	1.81394	23.2503	1.24878						
25.84922	1.8075	23.80578	1.25775						
26.40492	1.80228	24.36126	1.26619						
26.96064	1.79606	24.91674	1.27441						
27.51634	1.79094	25.47221	1.28228						
28.07205	1.78563	26.02769	1.29022						
28.62777	1.78256	26.58317	1.29778						
29.18348	1.77772	27.13865	1.30509						
29.73918	1.77272	27.69413	1.31234						
30.29489	1.76737	28.2496	1.31941						
30.85059	1.76241	28.80507	1.32609						
31.4063	1.75797	29.36055	1.33291						
31.962	1.75331	29.91602	1.33934						
32.5177	1.74891	30.4715	1.34559						
33.07341	1.74494	31.02699	1.35191						
33.4235	1.7345	31.58246	1.35775						
33.9792	1.72947	32.13794	1.36375						
34.53492	1.72491	32.69342	1.36956						
35.09062	1.72322	33.2489	1.37509						
35.64632	1.7195	33.80438	1.38063						
36.20203	1.71478	34.35985	1.38616						
36.75773	1.71034	34.91533	1.39134						
37.31344	1.70584	35.4708	1.39653						
37.86914	1.70125	36.02627	1.40141						
38.42485	1.69466	36.58175	1.40656						
38.98056	1.69116	37.13722	1.41162						
39.53626	1.68672	37.6927	1.41637						
40.09197	1.68231	38.24818	1.42128						
40.64768	1.67834	38.80365	1.42591						
41.20339	1.677	39.35913	1.43069						
41.75909	1.67409	39.91461	1.43528						
42.3148	1.67078	40.47009	1.43994						
42.8705	1.66625	41.02557	1.44456						
43.42621	1.66209	41.58106	1.44891						
43.98192	1.65809	42.13654	1.45347						
44.53763	1.65294	42.69201	1.458						
45.09333	1.64944	43.24749	1.46263						
45.64904	1.64966	43.80297	1.46691						
46.20475	1.64578	44.35844	1.47141						
46.76045	1.64084	44.91393	1.47556						
47.31616	1.63506	45.4694	1.47988						
47.87186	1.63197	46.02487	1.48409						
48.42757	1.62838	46.58035	1.48819						
48.98327	1.62481	47.13583	1.4925						
49.53897	1.62159	47.6913	1.49666						
50.09469	1.61991	48.24678	1.50094						
50.65039	1.61719	48.80226	1.50506						
51.20611	1.61375	49.35774	1.50913						
51.76183	1.61037	49.91321	1.51312						
52.31754	1.60775	50.46869	1.51753						
52.87324	1.60491	51.02417	1.52159						
53.42895	1.60194	51.57964	1.5255						
53.98466	1.59894	52.13512	1.52969						
54.54038	1.59591	52.6906	1.53366						
55.09608	1.59334	53.24607	1.53784						
55.65179	1.59016	53.80154	1.54188						
56.2075	1.59156	54.35702	1.54588						
56.76321	1.58834	54.9125	1.54997						
57.31892	1.58506	55.46797	1.55372						
57.87463	1.58225	56.02345	1.55775						
58.43033	1.57766	56.57892	1.56166						
58.98603	1.57506	57.13441	1.56569						
59.54174	1.57197	57.68988	1.56953						
60.09742	1.56866	58.24536	1.5735						
60.65312	1.56531	58.80084	1.57719						
61.20882	1.56284	59.3563	1.58106						
61.76451	1.56041	59.91178	1.58494						
62.3202	1.558	60.46725	1.58881						
62.8759	1.55591	61.02272	1.59234						
63.43159	1.55319	61.5782	1.59625						
63.98728	1.55025	62.13366	1.60013						
64.54297	1.54809	62.68913	1.60375						
65.09867	1.54541	63.2446	1.60763						
65.65437	1.54338	63.80007	1.61138						
66.21006	1.54081	64.35554	1.61488						
66.76576	1.53869	64.91101	1.61872						
67.32145	1.53616	65.46648	1.62225						
67.87714	1.534	66.02195	1.62588						
68.43284	1.53216	66.57742	1.62972						
68.98853	1.52988	67.1329	1.63338						
69.54422	1.52706	67.68836	1.63669						
70.09992	1.52497	68.24384	1.6405						
70.65561	1.52262	68.7993	1.64394						
71.21131	1.51984	69.35477	1.64769						
71.767	1.51744	69.91024	1.65113						
72.32268	1.51522	70.46572	1.65456						
72.87837	1.51241	71.02119	1.65816						
73.43407	1.51022	71.57666	1.66166						
73.98976	1.50756	72.13213	1.66494						
74.54545	1.50519	72.68761	1.6685						
75.10115	1.50366	73.24308	1.67175						
75.65684	1.50056	73.79855	1.67516						
76.21253	1.49831	74.35403	1.67841						
76.76821	1.49653	74.9095	1.68194						
77.3239	1.49391	75.46497	1.68522						
77.87959	1.49225	76.02044	1.68844						
78.43527	1.49012	76.57592	1.69191						
78.99098	1.4885	77.1314	1.69506						
79.54667	1.48572	77.68687	1.69831						
80.10236	1.48297	78.24234	1.70166						
80.65805	1.48097	78.79782	1.70509						
81.21374	1.47916	79.35329	1.70834						
81.76943	1.47741	79.90877	1.71159						
82.32512	1.47172	80.46424	1.71491						
82.88081	1.46663	81.01971	1.71797						
83.43651	1.46525	81.57517	1.72109						
83.99219	1.4625	82.13064	1.72441						
84.54788	1.45906	82.68611	1.72753						
85.10357	1.45672	83.24158	1.73081						
85.65925	1.45406	83.79705	1.73394						
86.21493	1.45169	84.35253	1.73713						
86.77062	1.44859	84.90799	1.74025						
87.32631	1.44613	85.46346	1.74344						
87.882	1.44422	86.01893	1.74663						
88.4377	1.44256	86.5744	1.74988						
88.99339	1.43947	87.12987	1.75322						
89.54908	1.43709	87.68535	1.75638						
90.10477	1.43459	88.24082	1.75969						
90.66046	1.43106	88.7963	1.76269						
91.21615	1.42847	89.35178	1.76594						
91.77184	1.42803	89.90724	1.76916						
92.32753	1.42728	90.46272	1.77231						
92.88322	1.42113	91.01819	1.77556						
93.43892	1.41969	91.57366	1.77869						
93.99461	1.41703	92.12913	1.78181						
94.55029	1.41481	92.6846	1.78494						
95.10598	1.41191	93.24007	1.78816						
95.66168	1.40984	93.79553	1.79137						
96.21738	1.40706	94.351	1.79462						
96.77307	1.40425	94.90646	1.79778						
97.32876	1.40203	95.46194	1.80116						
97.88444	1.39953	96.01741	1.80441						
98.44013	1.39731	96.57288	1.80753						
98.99582	1.39431	97.12834	1.81062						
99.55151	1.39156	97.68381	1.814						
100.1072	1.39028	98.23927	1.81728						
100.66289	1.38969	98.79473	1.82044						
101.21858	1.38766	99.35019	1.82363						
101.77428	1.3855	99.90566	1.82697						
102.32997	1.38241	100.46114	1.83016						
102.88566	1.37966	101.0166	1.83366						
103.44135	1.37688	101.57206	1.83681						
103.99704	1.37425	102.12752	1.84006						
104.55273	1.37147	102.68298	1.84331						
105.10843	1.36988	103.23844	1.84659						
105.66412	1.36722	103.79391	1.84991						
106.21981	1.36437	104.34936	1.85328						
106.7755	1.36241	104.90483	1.8565						
107.33119	1.35844	105.4603	1.85984						
107.88688	1.35634	106.01569	1.86312						
108.44257	1.35447	106.57115	1.86641						
108.99827	1.35103	107.12661	1.86975						
109.55396	1.34909	107.68208	1.87312						
110.10964	1.347	108.23754	1.87653						
110.66533	1.3435	108.793	1.87972						
111.22102	1.34169	109.34847	1.88316						
111.74337	1.33163	109.90394	1.88641						
112.29907	1.32941	110.45941	1.88972						
112.85476	1.3275	111.01487	1.89319						
113.41045	1.32544	111.57034	1.89644						
113.96614	1.32325	112.12581	1.89978						
114.52183	1.32019	112.68127	1.90328						
115.07752	1.31819	113.23673	1.90675						
115.63321	1.31659	113.7922	1.91						
116.18889	1.31344	114.34765	1.91325						
116.74458	1.31113	114.90312	1.91675						
117.30027	1.30784	115.45858	1.92006						
117.47254	1.29772	116.01404	1.92356						
118.02823	1.29591	116.5695	1.92691						
118.58391	1.29819	117.12496	1.93028						
119.13959	1.29475	117.68042	1.93359						
119.69529	1.28897	118.23588	1.93691						
120.25098	1.28606	118.79134	1.94038						
120.66774	1.27594	119.3468	1.94353						
121.22344	1.27525	119.90226	1.94713						
121.77913	1.27106	120.45772	1.95053						
122.33481	1.26737	121.01318	1.95381						
122.8905	1.26291	121.56864	1.95725						
123.44619	1.25819	122.1241	1.96066						
124.00188	1.253	122.67955	1.96378						
124.55757	1.25153	123.23501	1.96713						
125.11327	1.24472	123.79046	1.97053						
125.66896	1.24038	124.34593	1.97409						
126.22466	1.23478	124.90136	1.97725						
126.78034	1.23131	125.4568	1.98081						
127.33603	1.2305	126.01225	1.98425						
127.89172	1.22581	126.5677	1.98753						
128.4474	1.22209	127.12314	1.99075						
129.00309	1.22194	127.67857	1.99416						
156.65872	1.14044	128.23402	1.99744						
157.21441	1.13953	128.7895	2.00081						
157.7701	1.13603	129.34495	2.00413						
158.32579	1.13037	129.90041	2.00731						
158.88148	1.12959	130.45587	2.01062						
159.43718	1.12312	131.01133	2.01416						
159.99287	1.12037	131.56678	2.01734						
160.54856	1.11831	132.12224	2.02056						
161.10425	1.11516	132.6777	2.02372						
161.65994	1.11275	133.23315	2.02719						
162.21563	1.10984	133.78861	2.03044						
162.77131	1.10781	134.34407	2.03363						
163.327	1.10534	134.89953	2.03691						
163.88269	1.10294	135.455	2.04						
164.43838	1.10025	136.01044	2.0435						
164.99406	1.097	136.5659	2.0465						
165.54975	1.09497	137.12136	2.04963						
166.10543	1.09222	137.67682	2.05294						
166.66112	1.09053	138.23227	2.05578						
167.21681	1.08803	138.78773	2.05916						
167.77249	1.08534	139.34319	2.06231						
168.32817	1.08306	139.89864	2.06559						
168.88386	1.08103	140.4541	2.06862						
169.43955	1.07853	141.00955	2.07163						
169.99523	1.07644	141.56501	2.07463						
170.55092	1.074	142.12046	2.07794						
171.10661	1.07244	142.67591	2.08078						
171.6623	1.06963	143.23137	2.08403						
172.21798	1.067	143.78682	2.08725						
172.77366	1.06503	144.34228	2.09019						
173.32935	1.06994	144.89774	2.09322						
173.88504	1.06834	145.4532	2.09641						
174.44072	1.06578	146.00864	2.09944						
174.99641	1.06384	146.5641	2.1025						
175.5521	1.06116	147.11955	2.10541						
176.10778	1.05866	147.67502	2.10856						
176.66347	1.056	148.23048	2.1115						
177.21915	1.05472	148.78591	2.11456						
177.77483	1.052	149.34135	2.11778						
178.33051	1.04959	149.89682	2.12063						
178.88619	1.04706	150.45229	2.12363						
179.44188	1.04456	151.00776	2.12631						
179.99757	1.04259	151.56323	2.12966						
180.55325	1.04097	152.11868	2.13256						
181.10894	1.03903	152.67412	2.1355						
181.66463	1.03675	153.22959	2.13869						
182.22031	1.03394	153.78505	2.14172						
182.776	1.03159	154.34049	2.1445						
183.33169	1.02931	154.89594	2.14759						
183.88738	1.02688	155.45139	2.1505						
184.44306	1.02509	156.00683	2.15341						
184.99875	1.02306	156.56229	2.15644						
185.55443	1.02056	157.11773	2.15944						
186.11012	1.01838	157.6732	2.16228						
186.6658	1.01616	158.22864	2.16534						
187.22149	1.01375	158.78409	2.16803						
187.77718	1.01166	159.33954	2.17116						
188.33288	1.00978	159.895	2.17416						
188.88856	1.00784	160.45045	2.17703						
189.44425	1.00597	161.00592	2.17997						
189.99993	1.00406	161.56136	2.18291						
190.55562	1.00197	162.11682	2.18591						
191.11131	0.99969	162.67228	2.18878						
191.667	0.99875	163.22772	2.19166						
192.22268	0.99778	163.78318	2.1945						
192.77837	0.99584	164.33863	2.19747						
193.33406	0.99422	164.89408	2.20047						
193.88974	0.99231	165.44953	2.20338						
194.44544	0.99416	166.00499	2.20631						
195.00112	0.99269	166.56043	2.20922						
195.5568	0.99109	167.11588	2.21203						
196.11249	0.98938	167.67133	2.21506						
196.66819	0.98888	168.22678	2.21809						
197.22387	0.98697	168.78223	2.22106						
197.77954	0.98616	169.33768	2.22419						
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